Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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In everyday applications, corrosion varies by materials and solutions.
SEP does not require ageing, although it might be required in a specification calling up this standard. Please share this page: Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. R Baboian, Corrosion Tests and Standards: The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
Aatm standards require the test sample to asgm aged prior to testing, to simulate the precipitation that might occur during welding.
Intergranular Corrosion Testing: An Overview of ASTM A262
If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
Please specify the maximum allowable corrosion rate and any available data on the sensitizing aetm treatment performed. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
Test Samples Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the sample be a minimum of mm long.
From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using sstm equipment.
For an alloy that is not listed, look for an alloy with a similar composition to a listed alloy to determine the most suitable test. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away.
Alternatively, a welded test-piece in the as-welded condition may be tested.
ASTM A Intergranular Corrosion Testing and Analysis
Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on. The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult.
This means that carbide formation during welding is highly unlikely, and modern CRAs should easily pass one of these tests. ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
Both of these tests should be followed by water quenching. Where a bend test is required, the sample must be bent over a mandrel of a diameter related to the specimen diameter, without any cracking, as determined by inspection under a low power microscope and a microsection in any suspicious areas.
Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. This document also points out which alloys a26 tests are intended for, and recommends the most appropriate test when none is specified.
The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. Table 1 below shows the various methods for four common standards: Good material should have a corrosion rate substantially less than the threshold value.
Based on your materials, application, astn requirements, the other 4 methods provide specific focuses.
Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.
The specifications for bend testing are shown in Table 4. ASTM G28 does not require samples to be heat treated. The Huey test method C is only for molybdenum-free grades, such as L, as alloys with molybdenum show high rates of attack in this test.
Carbon and Sulfur Analysis. ASTM G28 was designed for nickel-based alloys, and a list of applicable alloys for methods A and B is in the standard.
Vickers Hardness 5Kg and 10Kg. ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods as follows: There are other requirements in these standards over details that are not discussed in this document, and these should be followed, such as conducting bend tests. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.
None of these are identical and cross substitution of results is not possible. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. ISO is specifically for a22 and all austenitic stainless steels, and recommends ageing at two different temperatures:. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.
All bend tests require a tensile test machine or similar, with suitable grips and sufficient strength to bend the strongest alloy. Selection of a Test Method The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult.
The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring aatm use.